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http://ir.nhri.org.tw/handle/3990099045/2713
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Title: | 2,2 '-diphenyl-1-picrylhydrazyl radical-scavenging active components from adlay (Coix lachryma-jobi L. var. ma-yuen Stapf) hulls |
Authors: | Kuo, CC;Chiang, WC;Liu, GP;Chien, YL;Chang, JY;Lee, CK;Lo, JM;Huang, SL;Shih, MC;Kuo, YH |
Contributors: | National Institute of Cancer Research |
Abstract: | An activity-directed fractionation and purification process was used to identify the antioxidative components of adlay hulls. Hulls of adlay (Coix lachryma-jobi L. var. ma-yuen Stapf) were extracted with methanol and then separated into water, 1-butanol, ethyl acetate, and hexane fractions. The 1-butanol-soluble fraction exhibited greater capacity to scavenge 2,2'-diphenyi-1-picryihydrazyl (DPPH) radicals when compared with fractions soluble in water, ethyl acetate, and hexane phases. The 1-butanol fraction was then subjected to separation and purification using Diaion HP-20 chromatography, silica gel chromatography, and HPLC. Six compounds showing strong antioxidant activity were identified by spectroscopic methods (H-1 NMR, C-13 NMR, IR, and MS) and by comparison with authentic samples to be coniferyl alcohol (1), syringic acid (2), ferulic acid (3), syringaresinol (4), 4-ketopinoresinol (5), and a new lignan, mayuenolide (6). |
Keywords: | Agriculture, Multidisciplinary;Chemistry, Applied;Food Science & Technology |
Date: | 2002-10-09 |
Relation: | Journal of Agricultural and Food Chemistry. 2002 Oct;50(21):5850-5855. |
Link to: | http://dx.doi.org/10.1021/jf020391w |
JIF/Ranking 2023: | http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=NHRI&SrcApp=NHRI_IR&KeyISSN=0021-8561&DestApp=IC2JCR |
Cited Times(WOS): | https://www.webofscience.com/wos/woscc/full-record/WOS:000178501300013 |
Cited Times(Scopus): | http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0037048523 |
Appears in Collections: | [張俊彥] 期刊論文 [郭靜娟] 期刊論文
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