國家衛生研究院 NHRI:Item 3990099045/2713
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    题名: 2,2 '-diphenyl-1-picrylhydrazyl radical-scavenging active components from adlay (Coix lachryma-jobi L. var. ma-yuen Stapf) hulls
    作者: Kuo, CC;Chiang, WC;Liu, GP;Chien, YL;Chang, JY;Lee, CK;Lo, JM;Huang, SL;Shih, MC;Kuo, YH
    贡献者: National Institute of Cancer Research
    摘要: An activity-directed fractionation and purification process was used to identify the antioxidative components of adlay hulls. Hulls of adlay (Coix lachryma-jobi L. var. ma-yuen Stapf) were extracted with methanol and then separated into water, 1-butanol, ethyl acetate, and hexane fractions. The 1-butanol-soluble fraction exhibited greater capacity to scavenge 2,2'-diphenyi-1-picryihydrazyl (DPPH) radicals when compared with fractions soluble in water, ethyl acetate, and hexane phases. The 1-butanol fraction was then subjected to separation and purification using Diaion HP-20 chromatography, silica gel chromatography, and HPLC. Six compounds showing strong antioxidant activity were identified by spectroscopic methods (H-1 NMR, C-13 NMR, IR, and MS) and by comparison with authentic samples to be coniferyl alcohol (1), syringic acid (2), ferulic acid (3), syringaresinol (4), 4-ketopinoresinol (5), and a new lignan, mayuenolide (6).
    关键词: Agriculture, Multidisciplinary;Chemistry, Applied;Food Science & Technology
    日期: 2002-10-09
    關聯: Journal of Agricultural and Food Chemistry. 2002 Oct;50(21):5850-5855.
    Link to: http://dx.doi.org/10.1021/jf020391w
    JIF/Ranking 2023: http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=NHRI&SrcApp=NHRI_IR&KeyISSN=0021-8561&DestApp=IC2JCR
    Cited Times(WOS): https://www.webofscience.com/wos/woscc/full-record/WOS:000178501300013
    Cited Times(Scopus): http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0037048523
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